Intergranular Corrosion Test (IGC) per ASTM A At TCR Engineering Services, several methods exist for the testing of intergranular corrosion. To conduct. Detecting Susceptibility to Intergranular Attack in Austenitic Stainless Steels. ASTM A is the specification which governs five practices used to determine if the. Abstract. A detailed study of AISI and stainless steels (SSs) has been conducted to correlate the degree of sensitization (DOS) measured by the.

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Due to the variance of attack in different materials, numerous methods Practices B-F are used to assess intergranular corrosion. Bend test criteria for several standards. Just remember that these tests were devised for specific groups of alloys and should not be applied to all CRAs! The test evaluates the resistance of extra-low-carbon steels to sensitization and intergranular attack from welding or heat treatment processes.

How do you select the right ASTM corrosion testing method for your material? The Huey test method C is only for molybdenum-free grades, such as L, as alloys with molybdenum show high rates of attack in this test.

The etch structure types used to classify the specimens are: The ASTM A tests can determine if the proper heat treatment was performed or if the alloys are in danger of intergranular corrosion occurring in use.

Wilson Hardness Conversion Chart. At the conclusion off the test, specimens are either visually examined or measured for weight loss and compared to an established astk rate for that specific material type.

Classification of structure then provides either acceptance or further testing required, which typically moves you to one of the next practices. Test Samples Samples may be rectangular or cylindrical to suit the test vessel, but where a bend test is required, it is suggested that the sample be a minimum of mm long.

Hence, it is normally only used for stainless steels intended for nuclear service, or another application involving nitric acid. ISO is specifically for duplex and all austenitic stainless steels, and recommends ageing at two different temperatures:. Vickers Hardness 5Kg and 10Kg. Some suggested criteria for the listed alloys are shown in Table 2, below.


The weight loss is calculated after each step, and reveals if the sample has been properly heat-treated. R Baboian, Corrosion Tests and Standards: Typical examination magnification is X to X. Rockwell or Superficial Hardness. This means that carbide formation during welding is highly unlikely, and modern CRAs should easily pass one of these tests. JavaScript is required for this astj.

Intergranular Corrosion Testing: An Overview of ASTM A262

A22 Oxalic Acid test is only used to ensure that no corrosion exists; samples are labeled either “Acceptable” or “Suspect”. All austenitic stainless steels should meet this requirement, if proper annealing took place. What is your typical turnaround time? View more articles about Aerospace Oil and Gas Transportation.

Intergranular simply means that the corrosion is taking place between the grains or crystals, which is where sigma phase or chromium carbides are going to form which makes the material susceptible to IGA. Awtm no specific test is specified, Table 5 suggests the most appropriate alongside a second choice, if the first is declined.

There are other requirements in these standards over details that are not discussed in this document, and these should be followed, such as conducting bend tests. As 15 hours is a difficult test period in practice, and is only a minimum, conducting the test for 20 hours overnight means that the two tests are equivalent.

Q262 tests do not provide a basis for predicting resistance to forms of corrosion other than intergranular, such as general corrosion, pitting, or stress-corrosion cracking. Metals like stainless steels and aluminum contain elements such as niobium and chromium, often integrated because of their natural corrosion resistance.

We provide intergranular corrosion evaluation, salt spray testing, stress corrosion, and various other methods to simulate exposure of your products or materials to corrosive environments. Make an Enquiry Notice: By using our website you consent to all cookies in accordance with our Cookie Policy.

Methods B and E are suggested for all grades of series austenitic alloys, while method F is suggested for cast type alloys. Methods for preparing the test specimens, rapid screening tests, apparatus setup and testing procedures, and calculations and report contents are described for each testing practice.


ASTM does not give any warranty express or implied or make any representation that the contents ashm this abstract are accurate, complete or up to date. ASTM G28 lists alloys and specifies the test exposure for each. Suggested test methods for different corrosion resistant alloys.

Practice A is a rapid screening examination of the microstructure to quickly determine if the structure is certain to be free of susceptibility to rapid intergranular attack.

Technical Resources

The level of corrosion is determined by mass loss. Intergranular corrosion occurs as a result of precipitation of nitridescarbidesand other intermetallic phasessuch as sigma phase, that occurs along the grain boundaries. The first and fastest step is the ASTM A Practice A, a rapid same-day screening method in Oxalic acid to determine the susceptibility to intergranular corrosion. The oxalic acid test is ast used before the Strauss test to determine if a sample is susceptible; samples that pass method A will generally show low corrosion rates in the Strauss test.

Awtm exception to this is ASTM G28 method A, where rates for the onset of intergranular corrosion are described in reference 1. A26 the correct method s rely on a complete understanding of your material and processes, as well as the concept of corrosion itself. This abstract is a brief summary of the referenced standard.

ASTM A Intergranular Corrosion Testing and Analysis

The Huey test works well to analyze chromium depleted regions and intermetallic precipitates, ast as sigma phase, and is also used for materials in strongly oxidizing environments such as nitric acid. The test solutions and exposures for some common intergranular corrosion tests.

ASTM A is a common intergranular corrosion testing method that can quickly screen batches of material to determine corrosion susceptibility.

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